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Short path distillation can be used to
ZZKD is a professional extraction solution manufacturer, Short path distillation is one of our main products and include: 2L short path distillation, 5L short path distillation, 10L short path distillation, 20L short path distillation,etc.
Short path distillation Fundamental:
Short-path distillation is carried out under high vacuum (<10Pa) conditions. The molecules evaporated on the heating surface reach the condensation surface as short as possible to be condensed, so as to realize the distillation process of liquid-liquid separation.When the distance between the heating surface and the condensation surface is less than or equal to the mean free path of the evaporated molecules, the distillation process is also called molecular distillation.Distillation process: the material enters the short-path distiller from the feed port,the distribution plate continuously and evenly distributes the materials to the vertical heating surface of the cylinder. While the materials fall by gravity, the rotating film scraping device forces a very thin liquid film on the heating surface.
Short path distillation performance characteristics:
High working vacuum and low distillation temperature;Large heat transfer coefficient and high evaporation efficiency;
The heating time is short, and the "no dead corner" design of the short-path distiller avoids the accumulation of materials on the distribution plate, heating surface and film-scraping system, and reduces the thermal polymerization and thermal decomposition of heat-sensitive substances.
Structural features:
The transmission device and mechanical seal of the short-path distiller are specially designed and manufactured to meet the long-term stable operation of high-precision equipment. The reduction ratio of the transmission device and the lubrication method of the mechanical seal are determined according to the working conditions and material characteristics of the short-path distiller ( Forced circulation lubrication, static lubrication) and mechanical seal cooling method.
The evaporating cylinder is integrally processed and formed without intermediate flange connection;
The inner surface of the cylinder has a high degree of smoothness and is not easy to stick to the material: the fine grinding surface finish can reach Ra0.8μm, and the special polishing finish can reach Ra0.2μm;
Unique design of liquid distributor and splash-proof device, effectively guaranteeing product quality;The high-precision design and manufacture of the short-path distiller can ensure the long-term stable operation of the device.There is almost no splash during the evaporation process. In most cases, the product requirements can be met even if there is no splash-proof device.When dealing with some special materials, the splash-proof device of the short-path still can more reliably guarantee the product quality;
A variety of film scrapers are available in a wide range of applications: oblique groove scraper type, roller type, metal hinge type, fixed scraper type, etc.
Applicable scope and typical applications:
Distillation, purification, concentration, and decolorization of petrochemical and chemical products; distillation and purification of heat-sensitive and easily oxidized chemical industrial products; distillation and separation of high-boiling point products.
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